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Liquid Chromatographic Tandem Mass Spectrometric (LC-MS/MS) Determination of Perfluorooctane Sulfonate (PFOS) and Perfluorooctanoic Acid (PFOA) in the Yolk of Poultry Eggs in Malaysia

Quoted values stay tied to the cited study. Empty sections are gaps.

Summary

Source-coded poultry yolk results retained with less-than symbols and footnotes.

Key numbers

Source-reported values checked against the cited page of the filed PDF. Values are reported as printed, without conversion. These are selected records, not an exhaustive transcription.

analytevalueunitbasissource locationlimits and qualifiers
PFOS0.64ng g−1 wwHome-produced chicken egg yolk; source 1PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10 ang g−1 wwHome-produced chicken egg yolk; source 1PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50ng g−1 wwHome-produced chicken egg yolk; source 2PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10ng g−1 wwHome-produced chicken egg yolk; source 2PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS0.50ng g−1 wwHome-produced chicken egg yolk; source 3PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10 ang g−1 wwHome-produced chicken egg yolk; source 3PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50 ang g−1 wwHome-produced chicken egg yolk; source 4PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10 ang g−1 wwHome-produced chicken egg yolk; source 4PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS1.01ng g−1 wwHome-produced chicken egg yolk; source 5PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10ng g−1 wwHome-produced chicken egg yolk; source 5PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS0.53ng g−1 wwHome-produced chicken egg yolk; source 6PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10 ang g−1 wwHome-produced chicken egg yolk; source 6PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50 ang g−1 wwHome-produced chicken egg yolk; source 7PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10 ang g−1 wwHome-produced chicken egg yolk; source 7PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50 ang g−1 wwHome-produced chicken egg yolk; source 8PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10ng g−1 wwHome-produced chicken egg yolk; source 8PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS0.52ng g−1 wwHome-produced chicken egg yolk; source 9PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10ng g−1 wwHome-produced chicken egg yolk; source 9PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50ng g−1 wwHome-produced chicken egg yolk; source 10PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10ng g−1 wwHome-produced chicken egg yolk; source 10PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50 ang g−1 wwDuck egg yolk; source 1PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10ng g−1 wwDuck egg yolk; source 1PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50 ang g−1 wwDuck egg yolk; source 2PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10ng g−1 wwDuck egg yolk; source 2PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50 ang g−1 wwDuck egg yolk; source 3PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10 ang g−1 wwDuck egg yolk; source 3PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50 ang g−1 wwQuail egg yolk; source 1PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10ng g−1 wwQuail egg yolk; source 1PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS0.69ng g−1 wwQuail egg yolk; source 2PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10ng g−1 wwQuail egg yolk; source 2PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50 ang g−1 wwQuail egg yolk; source 3PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10 ang g−1 wwQuail egg yolk; source 3PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOS<0.50 ang g−1 wwQuail egg yolk; source 4PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.
PFOA<0.10 ang g−1 wwQuail egg yolk; source 4PDF p.7 Table 3 and footnoteFootnote a: between LOD and LLOQ. PFOS LOD 0.1, LLOQ 0.5; PFOA LOD 0.02, LLOQ 0.1 ng g−1.

Evidence Fitness

Methods (brief)

Protein precipitation using acetonitrile followed by LC-MS/MS (PDF p.7 and methods pp.10 to 12).

Targets as printed or genericized: PFOS; PFOA (PDF p.7 Table 3).

Limitations

Yolk is not whole egg. The narrative sample total and displayed source groups are not reconciled by inference. The table omits commercial chicken sample rows mentioned in the narrative. No conversions, risk thresholds, representativeness claims, or safety conclusions are added.

Provenance notes

Local staged PDF copied unchanged. DOI checked in deposited PDF against MANIFEST; no external resolution attempted. Title and citation metadata checked against the PDF first page.

See the cell MISMATCHES.csv for unresolved discrepancies. The legacy MANIFEST analyte field is discovery metadata, not an audited target list.

Wiki pages updated on ingest

Eggs

PFOA

PFOS